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3-[5,6-Dimethyl-1,3-benzothiazol-2-yl)diazenyl]-1-methyl-2-phenyl-1H-indole

✍ Scribed by Hökelek, Tuncer ;Seferoğlu, Zeynel ;Şahin, Ertan

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
945 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 24 H 20 N 4 S, the phenyl ring forms a dihedral angle of 49.22 (7) with the indole ring system. The indole and benzothiazole ring systems are both approximately planar, with dihedral angles between the five-and sixmembered rings of 0.98 (7) and 1.28 (5) , respectively. They are also oriented relative to the central N N double bond at angles of 3.12 (14) and 3.82 (10) , respectively.

📜 SIMILAR VOLUMES

1,2-Dimethyl-3-[(5-methylsulfanyl-1,3,4-
1,2-Dimethyl-3-[(5-methylsulfanyl-1,3,4-thiadiazol-2-yl)diazenyl]-1H-indole
✍ Hökelek, Tuncer ;Seferoğlu, Zeynel ;Şahin, Ertan ;Ertan, Nermin 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 112 KB

The asymmetric unit of the title compound, C 13 H 13 N 5 S 2 , contains two molecules. The thiadiazole rings form dihedral angles of 4.19 (7) and 1.41 (7) with the indole ring systems in the two molecules.

2-(2,5-Dimethyl­benz­yl)-3-phenyl­sulfan
2-(2,5-Dimethyl­benz­yl)-3-phenyl­sulfan­yl-1-phenyl­sulfon­yl-1H-indole
✍ Usha, G. ;Selvanayagam, S. ;Velmurugan, D. ;Ravikumar, K. ;Sureshbabu, N. ;Srini 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 245 KB

In the title compound, C 29 H 25 NO 2 S 2 , the benzene rings of the phenylsulfonyl and the dimethylbenzyl substituents are almost perpendicular to the indole unit, whereas the dihedral angle between the phenyl rings of the phenylsulfanyl and phenylsulfonyl groups is 71.2 (1) . The molecules in the