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1,2-Dimethyl-3-[(5-methylsulfanyl-1,3,4-thiadiazol-2-yl)diazenyl]-1H-indole

✍ Scribed by Hökelek, Tuncer ;Seferoğlu, Zeynel ;Şahin, Ertan ;Ertan, Nermin

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
112 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

The asymmetric unit of the title compound, C 13 H 13 N 5 S 2 , contains two molecules. The thiadiazole rings form dihedral angles of 4.19 (7) and 1.41 (7) with the indole ring systems in the two molecules.

📜 SIMILAR VOLUMES

3-[5,6-Dimethyl-1,3-benzothiazol-2-yl)di
3-[5,6-Dimethyl-1,3-benzothiazol-2-yl)diazenyl]-1-methyl-2-phenyl-1H-indole
✍ Hökelek, Tuncer ;Seferoğlu, Zeynel ;Şahin, Ertan 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 945 KB

In the title compound, C 24 H 20 N 4 S, the phenyl ring forms a dihedral angle of 49.22 (7) with the indole ring system. The indole and benzothiazole ring systems are both approximately planar, with dihedral angles between the five-and sixmembered rings of 0.98 (7) and 1.28 (5) , respectively. They

2-{[3-(4-Chlorophenyl)-1,2,4-oxadiazol-5
2-{[3-(4-Chlorophenyl)-1,2,4-oxadiazol-5-yl]methylsulfanyl}-5-methyl-1,3,4-thiadiazole
✍ Wang, Pin-liang ;Li, Hai-ling ;Kang, Si-shun ;Wang, Hai-bo 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 266 KB

The title compound, C~12~H~9~ClN~4~OS~2~, was synthesized __via__ condensation of 5-chloromethyl-3-(4-chlorophenyl)-1,2,4-oxadiazole with 5-mercapto-2-methyl-1,3,4-thiadiazole. The benzene and oxadiazole rings are coplanar due to the extended aromatic system. The angle between this plane and the thi