✦ LIBER ✦

2H-1,2-Azaphosphindoles – Synthesis and Characterization

✍ Scribed by Victorio Cadierno; Bruno Donnadieu; Alain Igau; Jean-Pierre Majoral

Publisher: John Wiley and Sons
Year: 2000
Tongue: English
Weight: 260 KB
Volume: 2000
Category: Article
ISSN: 1434-1948
DOI: 10.1002/(sici)1099-0682(200003)2000:3<417::aid-ejic417>3.0.co;2-a

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✦ Synopsis

The first 1,2-azaphosphindoles 14a,b, 15a,b were obtained in a straightforward manner upon heating diphenylzirconocene in the presence of a cyanophosphane, which afforded azazirconacyclopentenes 11a,b which can be reacted with various dichlorophosphanes. The use of the tetrachlorodiphosphane Cl 2 P(CH 2 ) 2 PCl 2 instead of a dichlorophosphane allowed the Scheme 1. Synthesis of 2H-1,2-azaphosphole tungsten complexes 8

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