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(2E,4E)-1-(3-Nitrophenyl)-5-phenylpenta-2,4-dien-1-one

✍ Scribed by Patil, P. S. ;Teh, Jeannie Bee-Jan ;Fun, Hoong-Kun ;Razak, Ibrahim Abdul ;Dharmaprakash, S. M.

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
213 KB
Volume
63
Category
Article
ISSN
1600-5368

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πŸ“œ SIMILAR VOLUMES

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The title compound, C 18 H 16 O 2 , was prepared using literature procedures and crystallized from an acetone-toluene solution (50:50 v/v). The dihedral angle between the two aromatic rings is 9.28 (8) A ˚. The crystal packing is stabilized by van der Waals forces.

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Single-crystal X-ray study T = 105 K Mean '(C±C) = 0.002 A Ê R factor = 0.030 wR factor = 0.062 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C~17~H~12~Cl~2~O, crystallizes in a centrosymmetric space group. The dihedral angle between the two benzene rings is 24.7β€…(1)Β°. The crystal packing is characterized by non-classical Cβ€”H...O and Cβ€”H...Cl inter- and intramolecular hydrogen bonds.

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In the title compound, C 17 H 16 N 2 O 3 , the dihedral angle between the benzene rings is 1.56 (7) . The nitro group is coplanar with the attached benzene ring while the dimethylamino group is twisted slightly away from the attached benzene ring. A weak intramolecular C-HÁ Á ÁO hydrogen bond is pre