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(2,4-Dichloro­phen­yl)methanol

✍ Scribed by Bambagiotti-Alberti, Massimo ;Bruni, Bruno ;Di Vaira, Massimo ;Giannellini, Valerio

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
187 KB
Volume
63
Category
Article
ISSN
1600-5368

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The title compound, C 14 H 8 Cl 4 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The dihedral angle formed by the two benzene ring planes is 38.39 (7) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

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The title compound, C 13 H 8 Cl 2 N 2 , was prepared by reaction of o-phenylenediamine with 2,4-dichlorobenzaldehyde under reflux in ethanol. The dihedral angle between the benzimidazole system and the benzene ring is 42.00 (15) . In the crystal structure, intermolecular N-HÁ Á ÁN interactions are p

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The title compound, C~16~H~12~Cl~2~O, exhibits second-order nonlinear optical properties as it crystallizes in a non-centrosymmetric space group. The dihedral angle between the benzene rings is 34.02 (6)°. Intermolecular C—H...O interactions link the molecules to form chains along the __c__ axis.