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2-(2,4-Dichlorophenyl)-1H-benzimidazole

✍ Scribed by Jian, Fang-Fang ;Yu, Huan-Qing ;Qiao, Yuan-Biao ;Liang, Tong-Ling ;Zhao, Pu-Su

Publisher: International Union of Crystallography
Year: 2006
Tongue: English
Weight: 118 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536806053384

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✦ Synopsis

The title compound, C 13 H 8 Cl 2 N 2 , was prepared by reaction of o-phenylenediamine with 2,4-dichlorobenzaldehyde under reflux in ethanol. The dihedral angle between the benzimidazole system and the benzene ring is 42.00 (15) . In the crystal structure, intermolecular N-HÁ Á ÁN interactions are present. Bruker P4 diffractometer ! scans Absorption correction: none 2602 measured reflections 2602 independent reflections 1316 reflections with I > 2(I) max = 27.0 3 standard reflections every 100 reflections intensity decay: none

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2-(2,4-Dichloro­phen­yl)-1H-benzimidazole

✦ Synopsis

2-(2,4-Dichlorophenyl)-1H-benzimidazole