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2,3,5-Tri-O-acetyl-1-(2-chloro­ethyl)-β-d-ribofuran­ose

✍ Scribed by Constable, Edwin C. ;Housecroft, Catherine E. ;Mahmood, Azad ;Neuburger, Markus ;Schaffner, Silvia

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
206 KB
Volume
62
Category
Article
ISSN
1600-5368

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## Abstract A new simple 3‐step synthesis of 1‐O‐acetyl‐2,3,5‐tri‐O‐benzoyl‐β‐Dribofuranoside is described. D‐Ribose is methylated to 1‐O‐methylribofuranoside and the latter benzoylated to 1‐O‐methyl‐2,3,5‐tri‐O‐benzoyl‐D‐ribofuranoside. Acetolysis with a mixture of acetic acid, acetic anhydride an