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2-(Pyrrolidin-1-ylmethyl)isoindoline-1,3-dione

✍ Scribed by Sakthivel, P. ;Joseph, P. S. ;Sebastiyan, A. ;Suvaikin, M. Yosuva ;Ramesh, M.


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
698 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis


In the title compound, C~13~H~14~N~2~O~2~, the pyrrolidine ring adopts an envelope conformation. The crystal structure is stabilized by C—H...O and C—H...N hydrogen bonds.


📜 SIMILAR VOLUMES


2-(1-Naphth­yl)isoindoline-1,3-dione
✍ Li, Jian ;Liang, Zu-Pei ;Sun, Xiao-Zheng 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 143 KB
2-Ethyl­isoindoline-1,3-dione
✍ Liang, Zu-Pei ;Li, Jian 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 224 KB

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.006 A R factor = 0.045 wR factor = 0.113 Data-to-parameter ratio = 7.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2,2′-Methylenebis(isoindoline-1,3-dione)
✍ Jiang, Zhou ;Wang, Jun-Dong ;Lin, Mei-Jin ;Chen, Nai-Sheng ;Huang, Jin-Ling 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 310 KB

The title compound, C~17~H~10~N~2~O~4~, consists of two phthalimide units connected by a methylene bridge. The N—C—N bond angle is 110.64 (12)°. In the crystal structure, the dihedral angle between the two phthalimide units in one molecule is 88.96 (2)°. The crystal packing is stabilized by the π–π

2-(2-Hydroxy­ethyl)isoindoline-1,3-dione
✍ Liang, Zu-Pei ;Li, Jian 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 216 KB

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.003 A R factor = 0.043 wR factor = 0.112 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2-(2-Pyrid­yl)isoindoline-1,3-dione
✍ Liang, Zu-Pei ;Li, Jian 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 115 KB

In the title compound, C 13 H 8 N 2 O 2 , the phthalimide unit and the pyridine ring are each essentially planar. The dihedral angle between these two planar ring systems is 62.1 (3) .