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2-(2-Hydroxy­ethyl)isoindoline-1,3-dione

✍ Scribed by Liang, Zu-Pei ;Li, Jian

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
216 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.003 A R factor = 0.043 wR factor = 0.112 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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2-Ethyl­isoindoline-1,3-dione
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✍ Liang, Zu-Pei ;Li, Jian 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 224 KB

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.006 A R factor = 0.045 wR factor = 0.113 Data-to-parameter ratio = 7.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title molecule, C 10 H 8 N 2 0 4 , the phthalimide unit is essentially planar. In the crystal structure, weak intermolecular C-HÁ Á ÁO hydrogen bonds link molecules into one-dimensional chains.

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The crystal structure of the title compound, C 14 H 9 NO 3 , is stabilized by a weak O-HÁ Á ÁO hydrogen bond. The dihedral angle between the phthalimide and hydroxyphenyl planes is 71.8 (2) .

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✍ Liang, Zu-Pei ;Li, Jian 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 115 KB

In the title compound, C 13 H 8 N 2 O 2 , the phthalimide unit and the pyridine ring are each essentially planar. The dihedral angle between these two planar ring systems is 62.1 (3) .