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2-Methyl-4-(4-methyl-1-piperazinyl)-10H-thieno­[2,3-b][1,5]­benzodiazepine methanol solvate

✍ Scribed by Wawrzycka-Gorczyca, Irena ;Mazur, Liliana ;Koziol, Anna E.

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
153 KB
Volume
60
Category
Article
ISSN
1600-5368

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📜 SIMILAR VOLUMES

Polymorphic form II of 2-methyl-4-(4-met
Polymorphic form II of 2-methyl-4-(4-methyl-1-piperazinyl)-10H-thieno­[2,3-b][1,5]­benzodiazepine
✍ Wawrzycka-Gorczyca, Irena ;Koziol, Anna E. ;Glice, Magdalena ;Cybulski, Jacek 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 165 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.002 A Ê R factor = 0.033 wR factor = 0.096 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2,4-Bis(4-chlorophenyl)-2-methyl-2,3-dih
2,4-Bis(4-chlorophenyl)-2-methyl-2,3-dihydro-1H-1,5-benzodiazepine
✍ An, Li-Tao ;Ding, Fei-Qing ;Zou, Jian-Ping ;Lu, Xiao-Hua 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 989 KB

In the title compound, C 22 H 18 C l2 N 2 , the seven-membered heterocyclic ring is in a boat-shaped conformation. The molecules are linked by N-HÁ Á ÁN hydrogen bonding into one-dimensional chains along the [010] direction.

8-Methyl-6-(4-methyl­piperazin-1-yl)-11H
8-Methyl-6-(4-methyl­piperazin-1-yl)-11H-pyrido­[2,3-b][1,4]­benzodiazepine
✍ Spirlet, Marie-Rose ;Graulich, Amaury ;Liégeois, Jean-Francois 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 240 KB

The conformation of the title compound, C 18 H 21 N 5 , is very similar to that observed in other diaryldiazepine structures such as clozapine and clozapine dihydrobromide. NÐHÁ Á ÁH hydrogen-bond interactions result in the formation of a dimer.