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2-Methyl-4-(4-methyl­piperazin-1-yl)-10H-thieno­[2,3-b][1,5]­benzodiazepine methanol solvate monohydrate

✍ Scribed by Capuano, Ben ;Crosby, Ian T. ;Fallon, Gary D. ;Lloyd, Edward J. ;Yuriev, Elizabeth ;Egan, Simon J.

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
233 KB
Volume
59
Category
Article
ISSN
1600-5368

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📜 SIMILAR VOLUMES

8-Methyl-6-(4-methyl­piperazin-1-yl)-11H
8-Methyl-6-(4-methyl­piperazin-1-yl)-11H-pyrido­[2,3-b][1,4]­benzodiazepine
✍ Spirlet, Marie-Rose ;Graulich, Amaury ;Liégeois, Jean-Francois 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 240 KB

The conformation of the title compound, C 18 H 21 N 5 , is very similar to that observed in other diaryldiazepine structures such as clozapine and clozapine dihydrobromide. NÐHÁ Á ÁH hydrogen-bond interactions result in the formation of a dimer.

Polymorphic form II of 2-methyl-4-(4-met
Polymorphic form II of 2-methyl-4-(4-methyl-1-piperazinyl)-10H-thieno­[2,3-b][1,5]­benzodiazepine
✍ Wawrzycka-Gorczyca, Irena ;Koziol, Anna E. ;Glice, Magdalena ;Cybulski, Jacek 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 165 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.002 A Ê R factor = 0.033 wR factor = 0.096 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

8-Chloro-5-(4-methyl­piperazin-1-yl)-11H
8-Chloro-5-(4-methyl­piperazin-1-yl)-11H-pyrido­[2,3-b][1,5]­benzoxazepine. Erratum
✍ Dupont, Léon ;Liégeois, Jean-François 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 78 KB

In the paper by Dupont & Lie  geois [Acta Cryst. (2003), E59, o1962±o1963.], there is an error in the chemical name given in the title. The correct title is `8-Chloro-5-(4-methylpiperazin-1yl)pyrido[2,3-b][1,5]benzoxazepine'.