𝔖 Bobbio Scriptorium
✦   LIBER   ✦

[2-(Di­methyl­amino)­benzyl][(N–B)-2-(di­methyl­ammonio)­benzyl]­phenyl­borate

✍ Scribed by Tong, Hong-Bo ;Wei, Xue-Hong ;Liu, Dian-Sheng ;Huang, Shu-Ping

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
194 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

In the crystal structure of the title compound, C 24 H 29 BN 2 , the coordination around both the B and N atoms is distorted tetrahedral. The ®ve-membered ring adopts an envelope conformation, with the ¯ap atom, B, displaced by 0.629 (6) A Ê from the plane of the other four atoms.

📜 SIMILAR VOLUMES

{[N-Benzyl-N-(2-pyridyl)­amino]­methyl­e
{[N-Benzyl-N-(2-pyridyl)­amino]­methyl­ene}di­phenyl­phosphine oxide
✍ Cui, Da-Jun ;Zeng, Xianshun ;Leng, Xuebing ;Xu, Fengbo ;Zhang, Zhengzhi 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 183 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.047 wR factor = 0.120 Data-to-parameter ratio = 14.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Di­methyl(2-tri­methyl­silyl­ethyl)[(2-t
Di­methyl(2-tri­methyl­silyl­ethyl)[(2-tri­methyl­silyl­ethyl)­di­methyl­ammonio]­ammonium tetrakis­[3,5-bis­(tri­fluoro­methyl)­phenyl]­borate at 130 K
✍ Hassall, Kathryn ;White, Jonathan 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 147 KB

Single-crystal X-ray study T = 130 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.046 wR factor = 0.126 Data-to-parameter ratio = 11.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

4-(N,N-Di­methyl­amino)-3-(2,2-di­phenyl
4-(N,N-Di­methyl­amino)-3-(2,2-di­phenyl­ethenyl)­coumarin
✍ Usman, Anwar ;Razak, Ibrahim Abdul ;Fun, Hoong-Kun ;Chantrapromma, Suchada ;Zhao 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 330 KB

Single-crystal X-ray study T = 213 K Mean '(C±C) = 0.002 A Ê R factor = 0.054 wR factor = 0.141 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Bis­[N-(2,6-di­methyl­phenyl)­amino­phen
Bis­[N-(2,6-di­methyl­phenyl)­amino­phenyl­glyoximato-κ2N,N′]­nickel(II) di­methyl sulfoxide solvate
✍ Batı, Hümeyra ;Zülfikaroğlu, Ayşin ;Taş, Murat ;Çalışkan, Nezihe ;Soylu, Serkan 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 213 KB

In the title compound, [Ni(C 16 H 16 N 3 O 2 ) 2 ]ÁC 2 H 6 OS, the Ni II atom lies on a crystallographic centre of symmetry and its coordination geometry is distorted square-planar, involving four N atoms from two oxime ligands. The dimethyl sulfoxide solvent is disordered over a crystallographic tw