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2′-Chloro­acetophenone azine

✍ Scribed by Zhao, Pu-Su ;Guo, Huan-Mei ;Jian, Fang-Fang ;Zheng, Jian ;Xiao, Hai-Lian

Book ID
104487859
Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
138 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 16 H 14 Cl 2 N 2 , was prepared by the reaction of hydrazine with 2-chloroacetophenone at room temperature. The molecule has C 2 symmetry with the midpoint of the N-N bond lying on the twofold axis.

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The molecule of the title compound, C 16 H 16 N 2 O 2 , is located on a centre of inversion (at the midpoint of the N-N bond), so that only one half of the molecule is crystallographically independent, and it adopts a syn structure with respect to the methoxy group and the aldehyde H atom. The benze