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2-Amino-2-oxazolin-4-ones. I. Synthesis 1a

โœ Scribed by Howell, Charles F.; Quinones, Nicanor Q.; Hardy, Robert A.

Book ID
120391360
Publisher
American Chemical Society
Year
1962
Tongue
English
Weight
782 KB
Volume
27
Category
Article
ISSN
0022-3263

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The B-amino alcohol structural unit is a key component of many important natural and synthetic substances.

Synthesis of 4-carboethoxy-4-oxazolin-2-
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โœ Robert V. Hoffman; M.Catherine Johnson; John F. Okonya ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 297 KB

3-Nosyloxy-2-ketoesters, available from 2-ketoesters, react efficiently with methyl carbamate and tosic acid in refluxing toluene to provide 4-carboalkoxy-4oxazolin-2-ones in good yields (41-84%).