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2-(2,6-Diiso­propyl­phenyl­amino)­cyclo­hex-1-enyl phenyl ketone

✍ Scribed by Gui, Guo-Qiu ;Bao, Feng ;Lü, Xing-Qiang ;Wu, Qing ;Ng, Seik Weng

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
199 KB
Volume
61
Category
Article
ISSN
1600-5368

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2-[2-(2,6-Di­methyl­phenyl­amino)­phenyl
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The ortho-disubstituted aromatic ring in the title compound, C 27 H 32 N 2 , is twisted by 76.1 (1) with respect to the isopropylsubstituted ring and by 89.3 (1) with respect to the methylsubstituted ring. The amino N atom is linked intramolecularly to the imino N by a hydrogen bond [NÁ Á ÁN = 2.686

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The structure of the ®rst oligo 1,1-cyclopropane, C 24 H 24 , is reported. All the three-membered rings are gauche with respect to each other. The molecules are connected by a network of CÐHÁ Á ÁC interactions.

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✍ Baker, Robert J. ;Bettentrup, Helga ;Jones, Cameron 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 154 KB

The title compound, C 14 H 24 N + ÁI À , was formed by a Schiff base condensation of 2,6-diisopropylaniline and acetone, using GaI as a Lewis acid. A strong interaction from the iminium hydrogen NÐH to the iodide counter-ion is observed. The 1 H and 13 C NMR data are also reported.

Diiso­propyl 2-(2-benzoyl-1-phenyl­ethyl
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✍ Jeyabharathi, A. ;Ponnuswamy, M. N. ;Narasimhan, S. ;Velmathi, S. 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 181 KB

In the title compound, C 24 H 28 O 5 , the keto group is planar. Weak CÐHÁ Á ÁO hydrogen bonds play a signi®cant role in the crystal packing.