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1H detected 1H,15N correlation spectroscopy in rotating solids

✍ Scribed by B Reif; R.G Griffin

Book ID
108487756
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
305 KB
Volume
160
Category
Article
ISSN
1090-7807

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Inverse Detection and Heteronuclear Edit
Inverse Detection and Heteronuclear Editing in 1H–15N Correlation and 1H–1H Double-Quantum NMR Spectroscopy in the Solid State under Fast MAS
✍ Ingo Schnell; Benedikt Langer; Serge H.M. SΓΆntjens; Marcel H.P. van Genderen; Ri πŸ“‚ Article πŸ“… 2001 πŸ› Elsevier Science 🌐 English βš– 371 KB

Signal enhancement in heteronuclear correlation spectra as well as signal selection in 1 H experiments can be achieved through inverse, i.e., 1 H, detection in the solid state under fast MAS conditions. Using recoupled polarization transfer (REPT), a heteronuclear 1 H-15 N single-quantum correlation