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Three-dimensional 1H15N heteronuclear correlation-15N15N dilute spin-exchange solid-state NMR spectroscopy

โœ Scribed by B.S.Arun Kumar; S.J Opella


Book ID
107798509
Publisher
Elsevier Science
Year
1991
Weight
266 KB
Volume
95
Category
Article
ISSN
0022-2364

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Three-Dimensional 13C Shift/1Hโ€“15N Coupl
โœ Zhengtian Gu; Stanley J. Opella ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 83 KB

Triple-resonance experiments capable of correlating directly bonded and proximate carbon and nitrogen backbone sites of uniformly 13 C-and 15 N-labeled peptides in stationary oriented samples are described. The pulse sequences integrate cross-polarization from 1 H to 13 C and from 13 C to 15 N with