𝔖 Bobbio Scriptorium
✦   LIBER   ✦

1H and 13C NMR studies of 2-functionalized 5-(methylsulfonyl)-1-phenyl-1H-indoles

✍ Scribed by Olga Cruz-López; Miguel A. Gallo; Antonio Espinosa; Joaquín M. Campos

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
116 KB
Volume
45
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

The ^1^H and ^13^C NMR resonances of thirty 2‐functionalized 5‐(methylsulfonyl)‐1‐phenyl‐1__H__‐indoles were assigned completely and unequivocally using the concerted application of one‐ and two‐dimensional experiments (DEPT, gs‐HMQC and gs‐HMBC). Finally, the influence of the 2‐substituent of 5‐(methylsufonyl)‐1‐phenyl‐1__H__‐indoles on the carbon atoms of the indole moiety was estimated. Copyright © 2006 John Wiley & Sons, Ltd.

📜 SIMILAR VOLUMES

1H and 13C NMR study of 2-substituted ph
1H and 13C NMR study of 2-substituted phenyl methyl sulphides
✍ S. Perumal; R. Chandrasekaran; S. Selvaraj; M. Ganesan; D. A. Wilson 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 47 KB 👁 2 views

The 1 H and 13 C NMR spectra of seven 2-substituted phenyl methyl sulphides were measured and their chemical shifts assigned on the basis of two-dimensional NMR techniques such as H,H-COSY and C,H-COSY. The chemical shifts of these sulphides were correlated with the appropriate SCS values of monosub

13C and 1H NMR study of N-5′-methylsalic
13C and 1H NMR study of N-5′-methylsalicylideneanilines
✍ K. Kishore; D. N. Sathyanarayana; V. A. Bhanu 📂 Article 📅 1987 🏛 John Wiley and Sons 🌐 English ⚖ 297 KB

The "C and 'H NMR spectra of six N-5'-methylsalicylideneanilines have been studied. Correlations of the chemical shifts of C-a (azomethine carbon) and C-4' with the cr, F, R , crI and a: parameters have been examined for N-5'-methylsalicylideneanilines, and also for N-benzylideneanilines and N-salic

Benzodiazepine analogues. Part 19.1H and
Benzodiazepine analogues. Part 19.1H and 13C NMR spectroscopic studies of 2-phenyl-1,4- and 1,5-benzoheterazepinethione derivatives
✍ Malose J. Mphahlele; Perry T. Kaye 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 103 KB 👁 1 views

Selected 1,4-and 1,5-benzoheterazepinones, prepared by the Schmidt rearrangement of flavanone analogues, were converted to the corresponding thiolactam derivatives using phosphorus pentasulfide. The proton and carbon chemical shifts of the thiolactam derivatives are compared with those of their lact

1H, 3H and 13C NMR studies on porphobili
1H, 3H and 13C NMR studies on porphobilinogen
✍ J. N. S. Evans; P. E. Fagerness; N. E. Mackenzie; A. I. Scott 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 English ⚖ 470 KB 👁 1 views
1H and 13C two-dimensional NMR study of
1H and 13C two-dimensional NMR study of magainin 1
✍ Chin Yu; Ta-Horng Yang 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 318 KB

## Abstract The ^1^H and ^13^C NMR spectra of magainin 1, a sterilizing agent of the skin, were studied using two‐dimensional techniques. All the ^1^H and ^13^C NMR resonances were unambiguously determined from a combination of 2D homo‐ and heteronuclear NMR spectroscopy.

1H and 13C NMR study of 1-substituted is
1H and 13C NMR study of 1-substituted isatins and their corresponding 3-(dicyanomethylidene)indol-2-ones
✍ Martha S. Morales-Ríos; Pedro Joseph-Nathan 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 340 KB

## Abstract The assignments of the ^1^H and ^13^C NMR signals of 1‐substituted isatins and their corresponding 3‐(dicyanomethylidene)indol‐2‐ones were derived by analysis of the ^13^C^1^H spin coupling patterns and by inspection of the two‐dimensional C, H shift correlation spectra. Erroneous lite