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Benzodiazepine analogues. Part 19.1H and 13C NMR spectroscopic studies of 2-phenyl-1,4- and 1,5-benzoheterazepinethione derivatives

✍ Scribed by Malose J. Mphahlele; Perry T. Kaye

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
103 KB
Volume
38
Category
Article
ISSN
0749-1581

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✦ Synopsis

Selected 1,4-and 1,5-benzoheterazepinones, prepared by the Schmidt rearrangement of flavanone analogues, were converted to the corresponding thiolactam derivatives using phosphorus pentasulfide. The proton and carbon chemical shifts of the thiolactam derivatives are compared with those of their lactam precursors.

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