15N chemical shift and 15N-13C dipolar tensors for the peptide bond in [1-13C]glycyl[15N]glycine hydrochloride monohydrate
✍ Scribed by G.S Harbison; L.W Jelinski; R.E Stark; D.A Torchia; J Herzfeld; R.G Griffin
- Publisher
- Elsevier Science
- Year
- 1984
- Weight
- 286 KB
- Volume
- 60
- Category
- Article
- ISSN
- 0022-2364
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We demonstrate a dipolar-chemical shift correlation technique for sign-sensitive determination of the torsion angle in solid peptides and proteins under magic-angle spinning. The indirect dimension of the experiment is obtained by separate but synchronous evolution of the magnetization under the 15
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