𝔖 Bobbio Scriptorium
✦   LIBER   ✦

13C chemical shift and 13C-15N dipolar tensors for the peptide bond: [1-13C]glycyl[15N]glycine·HCl·H2O

✍ Scribed by R.E Stark; L.W Jelinski; D.J Ruben; D.A Torchia; R.G Griffin


Publisher
Elsevier Science
Year
1983
Weight
470 KB
Volume
55
Category
Article
ISSN
0022-2364

No coin nor oath required. For personal study only.


📜 SIMILAR VOLUMES


Long-range J(15N,13C) and J(13C,13C) cou
✍ Josef Jirman; Milan Nádvorník; Jana Sopková; Alexander Popkov 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 English ⚖ 211 KB 👁 1 views

Chiral synthons containing either 13Cor 15N-labelled glycine were prepared. The 13C and 15N NMR spectra of the Ni(II) complex of the Schi † base of (S)-2-(N-benzylprolyl)aminobenzophenone and 13C-1-, 13C-2or 15N-labelled glycine were measured and assigned. The observed splitting of the carbon signal

Determination of the Peptide Torsion Ang
✍ M. Hong; J.D. Gross; W. Hu; R.G. Griffin 📂 Article 📅 1998 🏛 Elsevier Science 🌐 English ⚖ 214 KB

We demonstrate a dipolar-chemical shift correlation technique for sign-sensitive determination of the torsion angle in solid peptides and proteins under magic-angle spinning. The indirect dimension of the experiment is obtained by separate but synchronous evolution of the magnetization under the 15

1H, 13C and 15N NMR chemical shifts of s
✍ Erkki Kolehmainen; Katri Laihia; Alexander V. Firsov; Vyacheslav I. Zayzev; Elen 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 90 KB

## Abstract ^1^H, ^13^C and ^15^N NMR chemical shifts of 10 substituted pyrazolo[1,5‐__a__]pyrimidines were assigned based on DQF ^1^H, ^1^H COSY, PFG ^1^H, ^13^C HMQC and PFG ^1^H,X (X = ^13^C and ^15^N) HMBC experiments and on literature data. Copyright © 2002 John Wiley & Sons, Ltd.

1H-, 13C-, and 15N-NMR chemical shifts f
✍ Jan Vícha; Michal Maloň; Petra Veselá; Otakar Humpa; Miroslav Strnad; Radek Mare 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 145 KB

## Abstract The ^1^H and ^13^C NMR resonances of 16 purine glucosides were assigned by a combination of one‐ and two‐dimensional NMR experiments, including gs‐COSY, gs‐HSQC, and gs‐HMBC, in order to characterize the effect of substituent and the position of glucose unit on the NMR chemical shifts.

Characterisation of uniformly 13C, 15N l
✍ Tatiana Egorova-Zachernyuk; Barth van Rossum; Cees Erkelens; Huub de Groot 📂 Article 📅 2008 🏛 John Wiley and Sons 🌐 English ⚖ 306 KB

## Abstract In this investigation we report a complete assignment of ^13^C, ^1^H and ^15^N solution and solid state chemical shifts of two bacterial photosynthetic pigments, bacteriochlorophyll (BChl) __a__ and bacteriopheophytin (BPheo) __a__. Uniform stable‐isotope labelling strategies were devel