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13C nuclear magnetic resonance study of some phosphinolipids: Assignments and conformational studies

✍ Scribed by Georg Kallinowski; Walter Vogt

Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
345 KB
Volume
27
Category
Article
ISSN
0749-1581

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✦ Synopsis

C chemical shifts and ''P,l'C spin-spin coupling constants are reported for six model phosphinates and eight synthetic phosphinolipids. The complex spectra of the synthetic phosphinolipids could be assigned from increments and couplings derived from the model compounds. Based on these investigations the '4PC) couplings of 7-15 Hz indicate a preferential truns orientation of the respective head-group carbon relative to the phosphorus. This behaviour is similar to that of natural phosphatidylcholine lipids.

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