The 13C NMR spectral data for 18 dihydropyrimidinediones and their 2-thio analogues are presented. The influence of substituents on the shielding of neighbouring atoms was analysed and the resonances were unambiguously assigned. 13C NMR spectroscopy was shown to be useful for structural determinatio
13C NMR Study of Terahydro–1,5–bezodiazepin–2–one Derivatives
✍ Scribed by B. D. Puodžiūnaitė; G. Mikulskienė; R. Jančienė; Z. Stumbrevičiūtė
- Publisher
- John Wiley and Sons
- Year
- 1996
- Tongue
- English
- Weight
- 137 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
13C NMR spectral data for nine tetrahydro-1.5-benzodiazepin-2-ones are reported and the chemical shift assignments are discussed. The steric energies of the E and Z isomers of formyl derivatives were estimated by computer molecular modeling
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