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13C NMR characterization of acetonitrile-hydroquinone clathrate

โœ Scribed by J.A. Ripmeester; J.S. Tse; D.W. Davidson

Publisher
Elsevier Science
Year
1982
Tongue
English
Weight
527 KB
Volume
86
Category
Article
ISSN
0009-2614

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โœฆ Synopsis

Proton-decoupled 13C spectm ofC~~~-~qumol clathnte generally confirm Mfak and Lee's "drstorted" X-my stmcture. The smgle-eryst~ spectn gw shwidiag antsotroplcs of 13 and 293 ppm for the CH3 and CN groups, rcspectweiy.

The CN triplet spbttmgs yrcld an mducct spur-spm coupling smsoiropy of ~430 Hz.

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