(1,2-Diaminocyclohexane)silver(I) trifluoromethanesulfonate
✍ Scribed by Usman, Anwar ;Fun, Hoong-Kun ;Zhu, Hai-Liang ;Wang, Xian-Jiang
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 307 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 152 K Mean '(C±C) = 0.009 A Ê R factor = 0.055 wR factor = 0.140 Data-to-parameter ratio = 21.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, {[Ag(bpe)](OTf)} n (OTf = tri¯uoromethanesulfonate) or {[Ag(C 12 H 12 N 2 )](CF 3 O 3 S)} n , has been prepared from the reaction of 1,2-bis(4-pyridyl)ethane (bpe) and Ag(CF 3 SO 3 ) in MeCN/H 2 O. The Ag I atom is twocoordinate in a slightly distorted linear arrangement, and the
The cations and anions in the title compound, C 18 H 22 BN 2 + ÁCF 3 SO 3 ## À , are connected by intermolecular CÐ HÁ Á ÁO hydrogen bonds, with HÁ Á ÁO distances between 2.34 and 2.60 A Ê , into layers parallel to the bc plane.