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10,11-Dihydro-10,11-dihydroxy-5H-dibenz[b,f]azepine-5-carboxamide, a metabolite of carbamazepine isolated from human and rat urine

✍ Scribed by Baker, K. M.; Csetenyi, J.; Frigerio, A.; Morselli, P. L.; Parravicini, F.; Pifferi, G.

Book ID
120985695
Publisher
American Chemical Society
Year
1973
Tongue
English
Weight
402 KB
Volume
16
Category
Article
ISSN
0022-2623

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The stereoselectivity of the reduction of 5-carbamoyl-l0, I 1-dihydro-1 l-oxo-SH-dibenz[bflazepine-lO-yl acetate (6), prepared in two steps from 10, I l-dihydro-lO-oxo-5H-dibenz[hflazepine-5-carboxamide (4), has been studied. Among the reagents used, diisobutylaluminum hydride (DIBAH) was found to g