𝔖 Bobbio Scriptorium
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1-[2-Hydroxy-4-(3-methylbut-2-enyloxy)phenyl]ethan-1-one

✍ Scribed by Cheng, Die ;Liu, Mo ;Liu, Deng-Ke ;Liu, Ying ;Liu, Chang-Xiao


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
424 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis


The title compound, C~13~H~16~O~3~, is an intermediate in the synthesis of the anti-ulcer agent sofalcone. The asymmetric unit contains two independent molecules. Intramolecular O—H...O hydrogen bonds are formed between the carbonyl and hydroxyl groups.


📜 SIMILAR VOLUMES


3-(2,4-Di­chloro­phenyl)-3-hydroxy-1-phe
✍ Yu, Zhifang ;Zhao, Bing ;Tian, Zhongzhen ;Gu, Xiuyan 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 214 KB

View of the molecule of (I), showing the atom-labeling scheme. Displacement ellipsoids are drawn at the 30% probability level.

Synthesis of 1-[2-hydroxy-4-(3-sulfo-1-p
✍ E. Koltai; K. Esses-Reiter; D. Bánfi 📂 Article 📅 1982 🏛 John Wiley and Sons 🌐 French ⚖ 258 KB 👁 1 views

## Abstract 1‐[2‐hydroxy‐4‐(3‐sulfo‐1‐propyloxy)‐phenyl]‐3‐ ‐(3‐hydroxy‐4‐methoxyphenyl)‐propan‐1‐one sodium salt labelled with ^14^C at its carbonyl group (__1__) was synthetized starting from sodium acetate‐1‐^14^C through acetyl chloride‐1‐^14^C, resacetophenone‐carbonyl‐^14^C (__2__), 2‐hydroxy

1-{4-[(E)-2-(9H-Carbazol-9-yl)ethenyl]ph
✍ Prukała, Wiesław ;Marciniec, Bogdan ;Kubicki, Maciej 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 852 KB

In the title molecule, C~22~H~17~NO, the two approximately planar carbazole and phenyl groups make a dihedral angle of 45.34 (5)°. In the crystal structure, C—H...O hydrogen-bonded dimers are connected by additional C—H...O and C—H...π interactions into chains along the [001] direction.