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Synthesis of 1-[2-hydroxy-4-(3-sulfo-1-propyloxy)-phenyl]- -3-(3-hydroxy-4-methoxyphenyl)-propan-1-one-1-14C sodium salt

✍ Scribed by E. Koltai; K. Esses-Reiter; D. Bánfi

Publisher
John Wiley and Sons
Year
1982
Tongue
French
Weight
258 KB
Volume
19
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

1‐[2‐hydroxy‐4‐(3‐sulfo‐1‐propyloxy)‐phenyl]‐3‐ ‐(3‐hydroxy‐4‐methoxyphenyl)‐propan‐1‐one sodium salt labelled with ^14^C at its carbonyl group (1) was synthetized starting from sodium acetate‐1‐^14^C through acetyl chloride‐1‐^14^C, resacetophenone‐carbonyl‐^14^C (2), 2‐hydroxy‐4‐(3‐sulfo‐1‐propyloxy)‐acetophenone‐carbonyl‐^14^C sodium salt (3) and 1‐[2‐hydroxy‐4‐(3‐sulfo‐1‐propyloxy)‐phenyl]‐3(3‐hydroxy‐4‐methoxyphenyl)‐2‐ propen‐1‐one‐1‐^14^C (4).

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