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π-Complexes of PdCl2 with 1,3-butadiene and 1,3-cyclooctadiene

✍ Scribed by M. Donati; F. Conti

Publisher: Elsevier Science
Year: 1966
Tongue: French
Weight: 215 KB
Volume: 7
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)72396-3

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✦ Synopsis

Althwgh the formation of ~4oaplorer betwoon olefins, and non-oonjugrtod dlolefiae, and PdO12 hae been known for 1210 No.11 Id5ntioal qualit5tiv5 ro5ult5 w5ro obtained br sllploying Iband rxohango on tho7t oomplor of PdCl~bonaonitrll5, and at511 core simply, by lotting palladium ohlorid5 to roaot alowly in the liquid diolofl~ at tha t5mparature5 reportad abov5. In thlr oa50, however, quantitative ~lold5 rib: not obtrimd ainoo not all tha PdClz 5mployod raaotad. No altoration or 15am~risation of the dlol5Sn in 5xoema ooonrred during tho5e proprcrtiona. The oomplor from 1,3-butac dimm and tht obtained from 1,4_oyoloootrdi5n5 prsoipitstad a5 hromwoolourod'orymtrlm fkom tha liquid diolofin! th5n they mope-

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