{[μ,η2-Bis(trimethylstannyl)]acetylene}hexacarbonyldicobalt
✍ Scribed by Zachwieja, Uwe ;Preut, Hans ;Mitchell, Terence ;Zavgorodnii, Vladislav S. ;Golosovskii, Andrei V. ;Klyuchinskii, Sergei A.
- Publisher
- International Union of Crystallography
- Year
- 2001
- Tongue
- English
- Weight
- 234 KB
- Volume
- 57
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.034 wR factor = 0.091 Data-to-parameter ratio = 21.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 200 K Mean '(C±C) = 0.012 A Ê R factor = 0.022 wR factor = 0.025 Data-to-parameter ratio = 10.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, [Fe 2 (C 14 H 17 NSSi)(CO) 6 ], was produced by the reaction of N-(3-thienylmethylidene)-4-(trimethylsilyl)aniline and Fe 2 (CO) 9 via a reaction sequence involving a CÐH activation step, followed by an intramolecular hydrogen transfer to the former imine C atom. The crystal stru
Single-crystal synchrotron study T = 160 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.054 wR factor = 0.135 Data-to-parameter ratio = 16.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 90 K Mean '(C±C) = 0.005 A Ê Disorder in solvent or counterion R factor = 0.034 wR factor = 0.089 Data-to-parameter ratio = 11.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.