Crystal growth and characterization of H
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W. Tao; L.M. Chen; X.M. Wang; C. Fan; W.P. Ke; X.G. Liu; Z.Y. Zhao; Q.J. Li; X.F
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Article
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2011
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Elsevier Science
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English
⚖ 851 KB
The bulk single crystals of S ¼ 1 chain compound Ni(C 3 H 10 N 2 ) 2 NO 2 ClO 4 are grown by using a slow evaporation method at a constant temperature and a slow cooling method. It is found that the optimum condition of growing large crystals is via slow evaporation at 25 1C using 0.015 mol NiðClO 4