(μ2-η2-2-tert-Butylethyn-1-yl)(μ2-chloro)bis{[bis(η5-cyclopentadienyl)dimethylsilane]titanium}
✍ Scribed by Kooijman, Huub ;Hogenbirk, Marijke ;Schat, Gerrit ;Akkerman, Otto S. ;Bickelhaupt, Friedrich ;Spek, Anthony L.
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 208 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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The title compound, 1,2-bis(4-nitrophenyl)ferrocene, [Fe(C 5 H 5 )(C 17 H 11 N 2 O 4 )], crystallizes with the planes of the two vicinal 4-nitrophenyl rings subtending angles of 46.04 (6) and 36.30 (7) at the plane of the substituted cyclopentadiene ring of the ferrocene moiety.
Single-crystal X-ray study T = 200 K Mean '(C±C) = 0.012 A Ê R factor = 0.022 wR factor = 0.025 Data-to-parameter ratio = 10.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.