μ-Oxo-bis{isopropoxo[2,2′-(methylenedithio)bis(6-tert-butyl-4-methylphenolato)]titanium(IV)}
✍ Scribed by Centore, Roberto ;Tuzi, Angela ;Capacchione, Carmine ;Oliva, Leone
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 104 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 173 K Mean (C-C) = 0.005 A Disorder in main residue R factor = 0.054 wR factor = 0.139 Data-to-parameter ratio = 21.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.004 A Ê R factor = 0.051 wR factor = 0.138 Data-to-parameter ratio = 13.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 22 H 36 N 2 O, contains piperidine as a major constituent. The two piperidine rings attached to the phenyl ring are in chair conformations. The structure is stabilized by van der Waals forces as well as OÐHÁ Á ÁN intramolecular hydrogen bonds.
Bis(tert-butylimido)[2-(dimethylaminomethyl)pyrrol-1-yl]tungsten(VI)-l-oxo-bis(tert-butylimido)-(g 2 -N,O-tert-butylnitroso)tungsten(VI)
Single-crystal synchrotron study T = 150 K Mean '(C±C) = 0.004 A Ê R factor = 0.084 wR factor = 0.228 Data-to-parameter ratio = 53.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.