α,α,4-Trichloro-α-phenyl-o-tolyl dichlorophosphinate
✍ Scribed by Pinkus, A. G. ;Klausmeyer, Kevin K. ;Feazell, Rodney P. ;Meng, Liliy Y. C.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 187 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.002 A Ê R factor = 0.025 wR factor = 0.071 Data-to-parameter ratio = 25.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 123 K Mean '(C±C) = 0.003 A Ê R factor = 0.026 wR factor = 0.063 Data-to-parameter ratio = 18.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The crystal structure of [RuCl 2 (C 13 H 13 N 3 ) 2 ] contains complexes on general positions and complexes located on crystallographic twofold rotation axes. The three independent 2-phenylazo-4,6-dimethylpyridine ligands all have the same conformation.
In the crystal structure of the title compound, [Co(NO 2 )-(C 44 H 28 N 4 )(H 2 O)]ÁCH 2 Cl 2 , the Co III atom has a distorted octahedral coordination, with the water molecule trans to the nitro ligand. The CoÐN(nitro) and CoÐO(aqua) bond distances are 1.863 (8) and 2.114 (8) A Ê , respectively. Th