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Über die Herstellung von N-Methyl-N-[1,2,3,4-tetra-hydro-naphtyl-(2)]-β-aminopropionsäure-(2′-oxy-isopropyl)-amid und N-Methyl-N-[1,2,3,4-tetrahydro-naphtyl-(2)]-β-amino-propionsäure-(2′-amino-isopropyl)-ester-dihydrochlorid

✍ Scribed by V. Burckhardt; W. Kündig; P. Sieber

Publisher
John Wiley and Sons
Year
1952
Tongue
German
Weight
449 KB
Volume
35
Category
Article
ISSN
0018-019X

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✦ Synopsis

Soci6t6 suisse de chimie, B&le -SocietA svizzera di chimica, Basilea. Nachdruck verboten. -Tous droits r6serv6s. -Printed in Switzerland. 181. uber die Herstellung von N-Methyl-N-[I, 2,3,4-tetrahydro-naphtyl-(2)] -P-aminopropionsaure-(2 ' -oxy-isopropyl) -amid und N-Methyl-N-[l, 2,3,4-tetrahydro-naphtyl-(2)] -P-amhopropionsaure-( 2'-amino-isopropyl)-ester-dihydrochlorid von V. Burckhardt, W. Kundig und P. Sieber. (19. IV. 52.) 1) Herr Prof. Dr. Hs. H . Gzinthard hat die Spektren aufgenommen und zusammen 2, G. 81, 587 (1951).

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## Abstract Sodium [1‐^14^C] isobutyrate: 1 was obtained by carbonation of isopropyl magnesium bromide with ^14^CO~2~. From: 1 [1‐^14^C] isobutyryl chloride: 3 was prepared, which through the successive actions of diazomethane and hydrogen bromide gave rise to 1‐bromo 3 methyl [2‐^14^C] 2‐butanone: