In this paper, we investigated electrical properties and microstructures of ZrTiO 4 (ZrO 2 -TiO 2 ) thin films prepared by the sol-gel method on ITO substrates at different annealing temperatures. All films exhibited ZrTiO 4 (1 1 1) and (1 0 1) orientations perpendicular to the substrate surface, an
ZrO2obtained by the sol-gel method: influence of synthesis parameters on physical and structural characteristics
β Scribed by M. L. Rojas -Cervantes; R. M. Martin -Aranda; A. J. Lopez -Peinado; J. De D. Lopez -Gonzalez
- Publisher
- Springer
- Year
- 1994
- Tongue
- English
- Weight
- 554 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0022-2461
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β¦ Synopsis
The effects of some synthesis parameters, such as alcohol/alcoxide and water/alcoxide molar ratios, type of solvent and reaction temperature, on the physical and crystalline characteristics of ZrO2 prepared by the sol-gel method were studied. The results show that gelling time, weight loss, surface area, pore-size distribution and crystalline phases were influenced by the preparation conditions.
π SIMILAR VOLUMES
Nano-rutile-titania has been synthesized via a sol-gel route using titanium tetra n-butoxide as the precursor and ethyl alcohol as the solvent at a low temperature of 80 β’ C. When synthesized with HCl as the catalyst, the powders crystallized without calcination, while the materials prepared using a