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(Z)-6-[(2-Methoxy­phenyl­amino)methyl­ene]-4-methyl­cyclo­hexa-2,4-dien-1(2H)-one monohydrate

✍ Scribed by Odabaşoğlu, Mustafa ;Albayrak, Çigdem ;Büyükgüngör, Orhan

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
155 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

2-Methoxyphenylamino)methylene]-4-methylcyclohexa-2,4-dien-1(2H)-one monohydrate Mustafa Odabas ¸og ˘lu, a * C ¸igdem Albayrak a and Orhan Bu ¨yu ¨kgu ¨ngo ¨rb

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4-[(4-Methyl­phenyl)­diazenyl]-6-methoxy
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The title compound, C 19 H 23 N 3 O 5 , adopts the keto±amine tautomeric form and the con®guration around the ÐN NÐ double bond is trans. There is an intramolecular NÐHÁ Á ÁO hydrogen bond and intermolecular OÐHÁ Á ÁO interactions, forming a three-dimensional network.

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4-[(3-Chloro­phenyl)­diazenyl]-6-methoxy-2-{[tris­(hydroxy­methyl)­methyl]­aminomethyl­ene}cyclo­hexa-3,5-dien-1(2H)-one
✍ Koşar, Başak ;Albayrak, Çigˇdem ;Odabaşoğlu, Mustafa ;Büyükgüngör, Orhan 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 220 KB

Single-crystal X-ray study T = 291 K Mean '(C±C) = 0.003 A Ê R factor = 0.043 wR factor = 0.116 Data-to-parameter ratio = 11.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

4-[(Z)-(4-Methoxy­anilino)­phenyl­methyl
4-[(Z)-(4-Methoxy­anilino)­phenyl­methyl­ene]-5-methyl-2-phenyl-2H-pyrazol-3(4H)-one
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Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.002 A Ê R factor = 0.040 wR factor = 0.124 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2-Hydr­oxy-6-[(2-hydroxy­phenyl­amino)me
2-Hydr­oxy-6-[(2-hydroxy­phenyl­amino)methyl­ene]cyclo­hexa­-2,4-dienone
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Bas ¸ak Kos ¸ar, a C ¸ig ˘dem Albayrak, b Mustafa Odabas ¸og ˘lu b and Orhan Bu ¨yu ¨kgu ¨ngo ¨ra \*

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The NH unit on the exocyclic C C double bond in the title compound, C 30 H 23 N 3 O, lies on the same side of the double bond as the carbonyl unit of the pyrazolonyl ring, and the two interact through an NÐHÁ Á ÁO hydrogen bond [2.671 (2) A Ê ].