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4-[(3-Chloro­phenyl)­diazenyl]-6-methoxy-2-{[tris­(hydroxy­methyl)­methyl]­aminomethyl­ene}cyclo­hexa-3,5-dien-1(2H)-one

✍ Scribed by Koşar, Başak ;Albayrak, Çigˇdem ;Odabaşoğlu, Mustafa ;Büyükgüngör, Orhan

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
220 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 291 K Mean '(C±C) = 0.003 A Ê R factor = 0.043 wR factor = 0.116 Data-to-parameter ratio = 11.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

4-[(4-Methyl­phenyl)­diazenyl]-6-methoxy
4-[(4-Methyl­phenyl)­diazenyl]-6-methoxy-2-{[tris­(hydroxy­methyl)­methyl]­amino­methyl­ene}cyclo­hexa-3,5-dien-1(2H)-one
✍ Koşar, Başak ;Albayrak, Çiğdem ;Odabaşoğlu, Mustafa ;Büyükgüngör, Orhan 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 183 KB

The title compound, C 19 H 23 N 3 O 5 , adopts the keto±amine tautomeric form and the con®guration around the ÐN NÐ double bond is trans. There is an intramolecular NÐHÁ Á ÁO hydrogen bond and intermolecular OÐHÁ Á ÁO interactions, forming a three-dimensional network.

4-[(Z)-(4-Methoxy­anilino)­phenyl­methyl
4-[(Z)-(4-Methoxy­anilino)­phenyl­methyl­ene]-5-methyl-2-phenyl-2H-pyrazol-3(4H)-one
✍ Bao, Feng ;Lü, Xing-Qiang ;Qiao, Yu-Qin ;Wu, Qing ;Ng, Seik Weng 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 186 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.002 A Ê R factor = 0.040 wR factor = 0.124 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.