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(Z)-2,3-Bis(3,4-di­methoxy­phenyl)-2-propen-1-ol

✍ Scribed by Stomberg, Rolf ;Albinsson, Bo ;Langer, Vratislav ;Li, Shiming ;Lundquist, Knut

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
239 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.107 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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(Z)-3-(3,4-Di­methoxy­phenyl)-2-(2-metho
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Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.101 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title compound, C 18 H 20 O 5 , the hydroxyl and dimethoxyphenyl substituents are in axial positions. The heterocyclic ring is in a half-chair conformation. The molecules are linked by OÐHÁ Á ÁO hydrogen bonds, leading to the formation of a chain extended throughout the whole of the crystal.

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Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.003 A Ê R factor = 0.051 wR factor = 0.123 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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✍ Yin, Qiang ;Zhang, Wen-Qin 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 416 KB

The title compound, C 26 H 30 O 7 , was obtained by the Grignard reaction of one molecule of 4-methoxybenzylmagnesium chloride with two molecules of 3,5-dimethoxybenzaldehyde. The two new chiral centers have the same absolute con®guration R (S), and the two hydroxyl groups, surrounded by the three b