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threo-2-(2,6-Di­methoxy­phenoxy)-1-(3,4-di­methoxy­phenyl)-1,3-propane­diol

✍ Scribed by Langer, Vratislav ;Lundquist, Knut ;Stomberg, Rolf ;Unge, Sverker von

Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
534 KB
Volume
58
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.003 A Ê R factor = 0.051 wR factor = 0.123 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the crystals of the title compound, C 19 H 24 O 8 , the molecules adopt a conformation in which the bulky 2,6-dimethoxyphenoxy and 4-hydroxy-3,5-dimethoxyphenyl groups are distant from each other. The O(phenoxy)ÐCÐCÐC(phenyl) torsion angle between these groups is À177.27 (10) . The conformation i

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✍ Langer, Vratislav ;Lundquist, Knut 📂 Article 📅 2001 🏛 International Union of Crystallography 🌐 English ⚖ 373 KB

Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.001 A Ê R factor = 0.044 wR factor = 0.124 Data-to-parameter ratio = 25.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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1-(2-Hydro­xy-4,6-di­methoxy-3-methyl­phenyl)-3-(4-methoxy­phenyl)-2-methyl-1,3-propane­dione
✍ Stomberg, Rolf ;Langer, Vratislav ;Hauteville, Marcelle 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 760 KB

Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.002 A Ê Disorder in main residue R factor = 0.049 wR factor = 0.144 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.101 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.