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X-ray, IR and 1H-NMR structural and conformational study of highly congested 2-alkyl-1,3-diols and of 3-(1-adamantyl)pentane-2,4-dione

✍ Scribed by M. Moreno-Mañas; J.F. Piniella; A. Alvarez-Larena; N. Galvez; M.E. Lloris; J. Marquet; A.C. Siani; G. Germain

Book ID
108372017
Publisher
Elsevier Science
Year
1992
Tongue
French
Weight
625 KB
Volume
48
Category
Article
ISSN
0040-4020

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## Abstract The ^1^H and ^13^C NMR resonances of 22 1‐alkyl‐pyrazole and 25 1‐alkyl‐pyrazoline derivatives were assigned completely using the concerted application of one‐ and two‐dimensional experiments (DEPT, gs‐HMQC and gs‐HMBC). Nuclear Overhauser enhancement (NOE) effects, conformational analy