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Vibrational spectra and conformations of 2-oxo-2-methyl-1,3,2-dioxaphosphorinane and 2-oxo-2-methyl-1,3,2-dioxaphosphepane molecules

✍ Scribed by R. R. Shagidullin; I. Kh. Shakirov; R. Kh. Musyakaeva; E. I. Matrosov

Book ID: 112449946
Publisher: Springer
Year: 1981
Tongue: English
Weight: 482 KB
Volume: 30
Category: Article
ISSN: 1573-9171
DOI: 10.1007/bf00963406

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I7O NMR chemical shifts of 2-oxo-1,3,2-dioxathiane and 13 of its methyl-substituted derivatives are reported. The chemical shifts depend strongly on temperature and to a much smaller extent on concentration. As a whole, however, they strongly support the predominance of chair conformations in these