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Use of Shift Reagent with MTPA Derivatives in 19F NMR Spectroscopy: Determination of Absolute Configuration of Stereomeric 2- and 3- Substituted Cyclohexanols

✍ Scribed by E. M. Merckx; A. J. Van De Wal; J. A. Lepoivre; F. C. Alderweireldt

Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
210 KB
Volume
87
Category
Article
ISSN
0037-9646

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Use of shift reagent with mtpa derivativ
Use of shift reagent with mtpa derivatives in 19F NMR spectroscopy: III. Determination of absolute configuration and enantiomeric purity of secondary alcohols
✍ A. J. De Van Wal; E. M. Merckx; G. L. LemiΓ¨re; T. A. van Osselaer; J. A. Lepoivr πŸ“‚ Article πŸ“… 2010 πŸ› Wiley (John Wiley & Sons) βš– 306 KB πŸ‘ 1 views

The LIS values produced by Eu(fodJ3 for the CF3-19F NMR signals of the MlTA e s t e r s of different stereoisomeric secondary alcohols have been measured. The applicability o f these values for assigning the absolute configuration of the alcohols has been studied. The advantages of t h i s method ov