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Use of controlled pore glass in solid phase oligosaccharide synthesis. Application to the semiautomated synthesis of a glyconucleotide conjugate

✍ Scribed by Matteo Adinolfi; Gaspare Barone; Lorenzo De Napoli; Alfonso Iadonisi; Gennaro Piccialli

Publisher: Elsevier Science
Year: 1998
Tongue: French
Weight: 233 KB
Volume: 39
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(98)00103-8

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✦ Synopsis

Three polymeric supports (polystyrene, Tentagel and controlled pore glass) have been tested far solid phase synthesis of oligosaccharides based on the trichloroacetimidate methodology. Controlled pore glass has been found to yield satisfactory results with TMSOTf as the glycosylation promoter. An application to the on-line preparation of a glyconucleotide is also reported.

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