Unusual dimerization of 1-ethyl-1,2,4-triazinium salts into 4a,4b,9,10-tetrahydro-1,3,6,8,8a,10a-hexaazaphenanthrenes
✍ Scribed by O.N. Chupakhin; B.V. Rudakov; S.G. Alexeev; V.N. Charushin; V.A. Chertkov
- Publisher
- Elsevier Science
- Year
- 1990
- Tongue
- French
- Weight
- 240 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0040-4039
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An efficient synthesis of novel spiro 2,3,7,8-tetrahydro-benzo[1,2-b:5,4-b 0 ]dipyran-4,6-dione and 2,3,8,9tetrahydro-benzo[1,2-b:4,3-b 0 ]dipyran-4,10-dione derivatives in high yields under microwave irradiation is described. The reaction was also studied under conventional heating conditions.