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Unexpected Recyclization of 1H-δ-Carbolines to Pyrrolo[1,2-a]indoles

✍ Scribed by S.Yu. Ryabova; L.M. Alekseeva; A.S. Shashkov; V.G. Granik

Book ID: 111548072
Publisher: Springer US
Year: 2003
Tongue: English
Weight: 164 KB
Volume: 39
Category: Article
ISSN: 0009-3122
DOI: 10.1023/a:1025110602750

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## Abstract Heating of 1′‐(__N__‐substituted carbamoyl)methylspiro[2__H__‐1‐benzopyran‐2,2′‐[2__H__]indoles] with potassium hydroxide in ethanol yields diastereomeric 5a,13‐methano‐6__H__‐1,3‐benzoxazepino[3,2‐__a__]indole‐12‐carbox‐amides. Reduction of the latter with sodium borohydride affords 1,