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Unexpected behaviour of a hexacoordinate silicon compound

✍ Scribed by F. Carré; C. Chuit; R.J.P. Corriu; A. Mehdi; C. Reyé

Book ID: 103229869
Publisher: Elsevier Science
Year: 1993
Tongue: English
Weight: 239 KB
Volume: 446
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(93)80054-f

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RSiR;: The suspension of 1 in ether was treated with an excess (3.6 equivalents) of organometallic reagent. After the addition, the mixture was refluxed for 1 h and then hydrolyzed with H2S04 (25%). The silane was then extracted as described above.