✦ LIBER ✦
Reaction of Grignard Reagents with Dianionic Hexacoordinated Silicon Complexes: Organosilicon Compounds from Silica Gel
✍ Scribed by Alain Boudin; Dr. Geneviève Cerveau; Dr. Claude Chuit; Prof. Dr. Robert J. P. Corriu; Dr. Catherine Reye
- Publisher
- John Wiley and Sons
- Year
- 1986
- Tongue
- English
- Weight
- 351 KB
- Volume
- 25
- Category
- Article
- ISSN
- 0044-8249
No coin nor oath required. For personal study only.
✦ Synopsis
RSiR;: The suspension of 1 in ether was treated with an excess (3.6 equivalents) of organometallic reagent. After the addition, the mixture was refluxed for 1 h and then hydrolyzed with H2S04 (25%). The silane was then extracted as described above.