𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Unexpected aspartimude formation during coupling reactions using Asp(OAl) in solid-phase peptide synthesis

✍ Scribed by Sandra C. Vigil-Cruz; Jane V. Aldrich


Book ID
105576549
Publisher
Springer Netherlands
Year
1999
Tongue
English
Weight
318 KB
Volume
6
Category
Article
ISSN
1573-3149

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


Use of Alloc-amino acids in solid-phase
✍ Nathalie Thieriet; Jordi Alsina; Ernest Giralt; FranΓ§ois GuibΓ©; Fernando Alberic πŸ“‚ Article πŸ“… 1997 πŸ› Elsevier Science 🌐 French βš– 286 KB

The use of Alloc group in SPPS for the N t~ protection of amino acids is an alternative to the Boc and Fmoc protecting groups. The smooth removal of Alloc group in neutral conditions with catalytic amounts of Pd(PPh3)4 in the presence of PhSiH3 as a scavenger for the allyl system permits orthogonali

A new micro-test for the detection of in
✍ W.S. Hancock; J.E. Battersby πŸ“‚ Article πŸ“… 1976 πŸ› Elsevier Science 🌐 English βš– 292 KB

A rapid micro-test using 2,4,6-trinitrobenzenesulphonic acid has been developed to detect incomplete coupling reactions in solid phase peptide synthesis. This new test will detect 3 nmol of free amino groups per milligram of resin.

New anchors useful in solid phase peptid
✍ Jean-Claude Alfred; Jean-Louis Aubagnac; Monique Calmes; Jacques Daunis; Btissan πŸ“‚ Article πŸ“… 1988 πŸ› Elsevier Science 🌐 French βš– 486 KB

A potyacrytIc resin oith NH2 funcffon8 uas made to react with o-bromoacetfc anhydrides with the viw of ffndfng new anchor8 use&Z In aottd phase peptide synthesis. Besides the normat aufde product, the process vfth Cz -bromopropfonic acfd anhydrfde gave rise to a d-akmtne derivattve whose structure w