A novel automatic system has been developed for the rapid solid-extraction and derivatization of different drugs and their metabolites from urine, prior to further analysis. Manual injection of underivatized/derivatized drugs in a GC/MS system, in which the quadrupole mass filter was operated conven
✦ LIBER ✦
‘Underflow’ introduction system for solid and liquid samples in bench-top gas chromatographic/mass spectrometric systems
✍ Scribed by Donata Favretto; Francesco Cecchinato; Pietro Traldi; Raymond E. March
- Publisher
- John Wiley and Sons
- Year
- 1995
- Tongue
- English
- Weight
- 319 KB
- Volume
- 30
- Category
- Article
- ISSN
- 1076-5174
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✦ Synopsis
Abstract
A simple, inexpensive inlet system was developed for the introduction of liquid and solid samples, to be employed in commercial gas chromatographic/mass spectrometric instruments, and not requiring sample injection through the chromatographic column. The system does not need any modifications of the ion source housing and pumping system and is based on admitting the sample vapour as an underflow to the normal helium flow through the chromatographic column at a location near the transfer line.
📜 SIMILAR VOLUMES
Rapid Solid-phase Extraction/Derivatizat
✍
Soledad Cárdenas; Mercedes Gallego; Miguel Valcárcel
📂
Article
📅
1997
🏛
John Wiley and Sons
🌐
English
⚖ 216 KB
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